Ústav technické a experimentální fyziky Institute of Experimental and Applied Physics

Coordination-Driven Self-Assembly on Polymer Surface for Efficient Synthesis of [Au(SPh)]n Coordination Polymer-Based Films

NázevTitle
Coordination-Driven Self-Assembly on Polymer Surface for Efficient Synthesis of [Au(SPh)]n Coordination Polymer-Based FilmsCoordination-Driven Self-Assembly on Polymer Surface for Efficient Synthesis of [Au(SPh)]n Coordination Polymer-Based Films
Druh výsledkuResult type
Článek v časopiseJournal article
AutořiAuthors
T. Tsuruoka, T. Ohhashi, J. Watanabe, O. Veselska
DOIDOI
10.1021/acs.cgd.9b01622
Časopis / citaceJournal / citation
Crystal Growth & Design. 2020, 20(3), 1961-1968. ISSN 1528-7505.
RokYear
2020
JazykLanguage
eng
WoSWoS
000518701900066
ScopusScopus
2-s2.0-85081167870
RIVRIV
RIV/68407700:21670/20:00337050!RIV21-MSM-21670___
ProjektProject
Institucionální podpora na rozvoj výzkumné org.Institucionální podpora na rozvoj výzkumné org.

AbstraktAbstract

We describe a simple bottom-up strategy to generate [Au(SPh)]n (SPh: thiophenolate) coordination polymer (CP) crystal-based thin films by employing an interfacial self-assembly on a nylon substrate. This method utilizes Au ion-doped nylon film as a precursor of [Au(SPh)]n CP, and a support substrate to control the kinetics of the reduction of Au ion from Au(III) to Au(I) and the complexation of Au(I) ions as well as SPh on the surface of the nylon film. The obtained CPs exhibit a fibril morphology with high crystallinity, which leads to a luminescent property. Further, we systematically study the formation mechanism of [Au(SPh)]n CPs on the substrates. Amorphous CPs formed at an early stage of reaction are transformed to crystalline CPs based on the re-arrangement of components during the reaction. The findings described herein offer novel and interesting openings for synthesis of Au ion-based CPs that demonstrate desired functions for a wide range of applications.

We describe a simple bottom-up strategy to generate [Au(SPh)]n (SPh: thiophenolate) coordination polymer (CP) crystal-based thin films by employing an interfacial self-assembly on a nylon substrate. This method utilizes Au ion-doped nylon film as a precursor of [Au(SPh)]n CP, and a support substrate to control the kinetics of the reduction of Au ion from Au(III) to Au(I) and the complexation of Au(I) ions as well as SPh on the surface of the nylon film. The obtained CPs exhibit a fibril morphology with high crystallinity, which leads to a luminescent property. Further, we systematically study the formation mechanism of [Au(SPh)]n CPs on the substrates. Amorphous CPs formed at an early stage of reaction are transformed to crystalline CPs based on the re-arrangement of components during the reaction. The findings described herein offer novel and interesting openings for synthesis of Au ion-based CPs that demonstrate desired functions for a wide range of applications.